Improvement in electrical, thermal and mechanical properties of epoxy by filling carbon nanotube

Улучшение электрических, тепловых и механических свойств эпоксидной смолы путем наполнения углеродными нанотрубками
Yinong Zhou, Ping‐Han Wu, Z.‐Y. Cheng, Jaronda Ingram, Shaik Jeelani
2008-01-01

dynamic mechanical analysiselectrical conductivityepoxy nanocompositefracture toughnessmulti-walled carbon nanotubes
In this study, electrical, thermal and mechanical properties of multi-walled carbon nanotubes (CNTs) reinforced Epon 862 epoxy have been evaluated.Firstly, 0.1, 0.2, 0.3, and 0.4 wt% CNT were infused into epoxy through a high intensity ultrasonic liquid processor and then mixed with EpiCure curing agent W using a high speed mechanical agitator.Electric conductivity, dynamic mechanical analysis (DMA), three point bending tests and fracture tests were then performed on unfilled, CNT-filled epoxy to identify the loading effect on the properties of materials.Experimental results show significant improvement in electric conductivity.The resistivity of epoxy decreased from 10 14 Ω•m of neat epoxy to 10 Ω•m with 0.4% CNT.The experimental results also indicate that the frequency dependent behavior of CNT/epoxy nanocomposite can be modeled by R-C circuit, permittivity of material increase with increasing of CNT content.DMA studies revealed that filling the carbon nanotube into epoxy can produce a 90% enhancement in storage modulus and a 17°C increase in Tg.Mechanical test results showed that modulus increased with higher CNT loading percentages, but the 0.3 wt% CNT-infusion system showed the maximum strength and fracture toughness enhancement.The decrease in strength and fracture toughness in 0.4% CNT/epoxy was attributed to poor dispersions of nanotubes in the composite.
1
Adding 0.4 wt% multi-walled carbon nanotubes reduced epoxy resistivity from 10^14 Ω·m to 10 Ω·m, substantially improving electrical conductivity.
2
At 0.4 wt% CNT, strength and fracture toughness decreased because nanotube dispersion was poor.
3
CNT incorporation increased storage modulus by 90% and raised the glass-transition temperature by 17°C.
4
CNT/epoxy frequency-dependent electrical behavior was modeled using an R-C circuit, while permittivity increased with CNT content.
5
Elastic modulus increased with CNT loading, but 0.3 wt% CNT produced the greatest improvements in strength and fracture toughness.

Multi-walled carbon nanotube-reinforced Epon 862 epoxy nanocomposites

The effects of CNT loading on the electrical, thermal, dynamic-mechanical, strength, and fracture-toughness properties of the epoxy nanocomposites

Publication Details
Publication Date
2008-01-01
Journal
Publisher
ISSN
Access Type
Author Information
Authors
Yinong Zhou
Ping‐Han Wu
Z.‐Y. Cheng
Jaronda Ingram
Shaik Jeelani
Explore further
Open the scid.ai AI chat with a ready-made request: it will find papers on a similar topic and help build a literature review.
Find similar papers in the chat
Make a presentation
100%