Microstructural characterization and properties of selective laser melted maraging steel with different build directions

Микроструктурная характеристика и свойства мартенситно-стареющей стали, наплавленной селективным лазерным плавлением, при различных направлениях построения
Kesong Zhou, Chaolin Tan, Wenyou Ma, Tongchun Kuang, Min Kuang
2018-10-22

Ni3X nanoprecipitates (X = Ti, Al, Mo)Orowan bowing mechanismbuild orientation / layer-wise effectmaraging steel 300selective laser melting
A nearly fully dense grade 300 maraging steel was fabricated by selective laser melting (SLM) additive manufacturing with optimum laser parameters. Different heat treatments were elaborately applied based on the detected phase transformation temperatures. Microstructures, precipitation characteristics, residual stress and properties of the as-fabricated and heat-treated SLM parts were systematically characterized and analyzed. The observed submicron grain size (0.31 μm on average) suggests an extremely high cooling rate up to 107 K/s. Massive needle-shaped nanoprecipitates Ni3X (X = Ti, Al, Mo) are clearly present in the martensitic matrix, which accounts for the age hardening. The interfacial relations between the precipitate and matrix are revealed by electron microscopy and illustrated in detail. Strengthening mechanism is explained by Orowan bowing mechanism and coherency strain hardening. Building orientation-based mechanical anisotropy, caused by ‘layer-wise effect’, is also investigated in as-fabricated and heat-treated specimens. The findings reveal that heat treatments not only induce strengthening, but also significantly relieve the residual stress and slightly eliminate the mechanical anisotropy. In addition, comprehensive performance in terms of Charpy impact test, tribological performance, as well as corrosion resistance of the as-fabricated and heat-treated parts are characterized and systematically investigated in comparison with traditionally produced maraging steels as guidance for industry applications.
1
Age hardening is caused by massive needle-shaped Ni3X (X = Ti, Al, Mo) nanoprecipitates within a martensitic matrix.
2
As-fabricated and heat-treated SLM parts were systematically evaluated for Charpy impact, tribological performance, and corrosion resistance versus conventionally produced maraging steels to inform industrial application.
3
Heat treatments both increase strength and substantially relieve residual stress while modestly reducing build-orientation mechanical anisotropy from the layer-wise effect.
4
Precipitate–matrix interfacial relationships were characterized by electron microscopy and underpin strengthening via Orowan bowing and coherency strain hardening.
5
SLM produced nearly fully dense grade 300 maraging steel with submicron average grain size of 0.31 μm, implying cooling rates up to 10^7 K/s.

Selective laser melted (SLM) grade 300 maraging steel parts fabricated with different build directions (as-fabricated and heat-treated specimens)

Microstructural features (grain size, martensitic matrix, Ni3X nanoprecipitates and interfaces), residual stress, strengthening mechanisms (Orowan bowing, coherency strain), mechanical anisotropy related to build orientation, and resulting mechanical, tribological, impact and corrosion properties

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2018-10-22
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Kesong Zhou
Chaolin Tan
Wenyou Ma
Tongchun Kuang
Min Kuang
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