Facile synthesis and application of Ag-chemically converted graphene nanocomposite

Простая синтез и применение нанокомпозита Ag–химически восстановленного графена
Min Shi, Bo Yan, Na Li, Mingxin Ye, Jianfeng Shen, Hongwei Ma, Yizhe Hu
2010-04-17

Ag-chemically converted graphenechemically converted graphenein situ chemical synthesissilver nanoparticlessurface-enhanced Raman scattering
An in situ chemical synthesis approach has been employed to prepare an Ag-chemically converted graphene (CCG) nanocomposite. The reduction of graphene oxide sheets was accompanied by generation of Ag nanoparticles. The structure and composition of the nanocomposites were confirmed by means of transmission electron microscopy (TEM), atomic force microscopy (AFM) and X-ray diffraction. TEM and AFM results suggest a homogeneous distribution of Ag nanoparticles (5–10 nm in size) on CCG sheets. The intensities of the Raman signals of CCG in such nanocomposites are greatly increased by the attached silver nanoparticles, i.e., there is surface-enhanced Raman scattering activity. In addition, it was found that the antibacterial activity of free Ag nanoparticles is retained in the nanocomposites, which suggests they can be used as graphene-based biomaterials.
1
An in situ chemical synthesis method produced Ag–chemically converted graphene (CCG) nanocomposites by simultaneous reduction of graphene oxide and generation of Ag nanoparticles.
2
Attached silver nanoparticles greatly increase the Raman signal intensities of CCG, indicating surface-enhanced Raman scattering activity.
3
TEM and AFM show homogeneous distribution of Ag nanoparticles of 5–10 nm size on CCG sheets.
4
The antibacterial activity of free Ag nanoparticles is retained in the Ag–CCG nanocomposites, supporting their potential use as graphene-based biomaterials.
5
X-ray diffraction, TEM, and AFM confirm the structure and composition of the Ag–CCG nanocomposites.

Ag-chemically converted graphene (CCG) nanocomposite consisting of chemically reduced graphene oxide sheets decorated with Ag nanoparticles

Structural, compositional, and functional properties including nanoparticle distribution (5–10 nm), enhanced Raman (surface-enhanced Raman scattering) due to Ag attachment, and retained antibacterial activity of the Ag‑CCG nanocomposite

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2010-04-17
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Authors
Min Shi
Bo Yan
Na Li
Mingxin Ye
Jianfeng Shen
Hongwei Ma
Yizhe Hu
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