Nuclear-Magnetic-Resonance Measurements Reveal the Origin of the Debye Process in Monohydroxy Alcohols

Измерения методом ядерного магнитного резонанса выявляют происхождение дебаевского процесса в моноатомных спиртах
Wolf Hiller, E. A. Rössler, Catalin Gainaru, R. Böhmer, R. Meier, S. Schildmann, Christina Lederle
2010-12-16

Debye processHydrogen-bonded glass-forming liquidsMonohydroxy alcoholsNuclear magnetic resonanceSpin-lattice relaxation
Monohydroxy alcohols show a structural relaxation and at longer time scales a Debye-type dielectric peak. From spin-lattice relaxation experiments using different nuclear probes, an intermediate, slower-than-structural dynamics is identified for n-butanol. Based on these findings and on translational diffusion measurements, a model of self-restructuring, transient chains is proposed. The model is demonstrated to explain consistently the so-far puzzling observations made for this class of hydrogen-bonded glass forming liquids.
1
Spin-lattice relaxation experiments with different nuclear probes identify an intermediate dynamics in n-butanol that is slower than structural relaxation.
2
The proposed model consistently accounts for previously puzzling observations in hydrogen-bonded glass-forming monohydroxy alcohols.
3
The self-restructuring transient-chain model explains the long-time Debye-type dielectric peak in monohydroxy alcohols.
4
Translational diffusion measurements, combined with nuclear-magnetic-resonance results, support a model of transient chains that continually self-restructure.

Hydrogen-bonded monohydroxy alcohol glass-forming liquids, specifically n-butanol

the intermediate slower-than-structural dynamics and its relationship to the Debye-type dielectric relaxation, interpreted through transient self-restructuring chains

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2010-12-16
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Authors
Wolf Hiller
E. A. Rössler
Catalin Gainaru
R. Böhmer
R. Meier
S. Schildmann
Christina Lederle
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